4C2W
Crystal structure of Aurora B in complex with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.922, 66.656, 116.903 |
Unit cell angles | 90.00, 96.83, 90.00 |
Refinement procedure
Resolution | 43.770 - 1.700 |
R-factor | 0.15841 |
Rwork | 0.156 |
R-free | 0.19534 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.020 |
RMSD bond angle | 2.198 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.600 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.030 | 0.140 |
Number of reflections | 74825 | |
<I/σ(I)> | 30.8 | 10 |
Completeness [%] | 97.1 | 94 |
Redundancy | 5.7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |