4BSU
Structure of the ectodomain of LGR5 in complex with R-spondin-1 (Fu1Fu2) in C2 crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 495.130, 62.150, 104.869 |
| Unit cell angles | 90.00, 91.19, 90.00 |
Refinement procedure
| Resolution | 65.501 - 3.200 |
| R-factor | 0.2425 |
| Rwork | 0.240 |
| R-free | 0.28750 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.246 |
| Refinement software | PHENIX ((PHENIX.REFINE: 1.8.2_1309)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 97.200 |
| High resolution limit [Å] | 3.200 |
| Rmerge | 0.080 |
| Number of reflections | 52878 |
| <I/σ(I)> | 7.1 |
| Completeness [%] | 99.0 |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
