4BQ7
Crystal structure of the RGMB-Neo1 complex form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 32 1 2 |
Unit cell lengths | 109.690, 109.690, 187.930 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 84.779 - 6.601 |
R-factor | 0.2561 |
Rwork | 0.254 |
R-free | 0.27990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.934 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 6.800 |
High resolution limit [Å] | 6.600 | 6.600 |
Rmerge | 0.230 | 0.790 |
Number of reflections | 2508 | |
<I/σ(I)> | 7.5 | 2.3 |
Completeness [%] | 97.7 | 97.4 |
Redundancy | 6 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1 M TRIS-HCL, PH 8.5, 0.2 M LITHIUM SULPHATE, 25 % PEG3350 |