4BOY
Structure of GAPDH from Thermosynechococcus elongatus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-02 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 141.920, 141.920, 76.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.960 - 2.150 |
R-factor | 0.16815 |
Rwork | 0.166 |
R-free | 0.20148 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3b1j |
RMSD bond length | 0.019 |
RMSD bond angle | 1.960 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.960 | 2.170 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.100 | 0.730 |
Number of reflections | 42473 | |
<I/σ(I)> | 9.58 | 2.26 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 6.22 | 6.05 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |