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4BOS

Structure of OTUD2 OTU domain in complex with Ubiquitin K11-linked peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]287
Detector technologyCCD
DetectorADSC CCD
Spacegroup nameP 6
Unit cell lengths164.480, 164.480, 44.730
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution44.730 - 2.350
R-factor0.1892
Rwork0.187
R-free0.23790
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4boq
RMSD bond length0.009
RMSD bond angle1.139
Data reduction softwareMOSFLM
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]53.8402.430
High resolution limit [Å]2.3502.350
Rmerge0.1200.890
Number of reflections29294
<I/σ(I)>101.9
Completeness [%]100.0100
Redundancy6.16.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
121% PEG 3,350, 100 MM SODIUM ACETATE, 200 MM MAGNESIUM NITRATE, PH 5.6

222036

PDB entries from 2024-07-03

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