4BM1
CRYSTAL STRUCTURE OF MANGANESE PEROXIDASE 4 FROM PLEUROTUS OSTREATUS - CRYSTAL FORM I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-06 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 1 |
Unit cell lengths | 39.990, 75.370, 75.610 |
Unit cell angles | 69.75, 75.69, 75.82 |
Refinement procedure
Resolution | 38.148 - 1.098 |
R-factor | 0.132 |
Rwork | 0.131 |
R-free | 0.14730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fmu |
RMSD bond length | 0.016 |
RMSD bond angle | 1.710 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.160 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.050 | 0.540 |
Number of reflections | 271193 | |
<I/σ(I)> | 13.5 | 1.9 |
Completeness [%] | 83.9 | 43 |
Redundancy | 13.5 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M NA-CITRATE AT PH 5.5 & 2.0 M (NH4)2SO4. |