4BJ1
Crystal structure of Saccharomyces cerevisiae RIF2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-08-17 |
| Detector | MARRESEARCH |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 78.360, 78.360, 236.210 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.650 - 2.940 |
| R-factor | 0.1986 |
| Rwork | 0.197 |
| R-free | 0.22860 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.160 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | SHARP |
| Refinement software | BUSTER (2.11.4) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.500 | 2.950 |
| High resolution limit [Å] | 2.940 | 2.940 |
| Rmerge | 0.050 | 0.540 |
| Number of reflections | 9796 | |
| <I/σ(I)> | 23.8 | 3.4 |
| Completeness [%] | 99.7 | 99.7 |
| Redundancy | 7.9 | 8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 14-20% 1,4-BUTANEDIOL, 100 MM NA ACETATE PH 5.1 |
