4BHK
Crystal Structure of Moss Leafy bound to DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-10 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.722, 84.523, 152.424 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.550 - 2.320 |
R-factor | 0.1984 |
Rwork | 0.196 |
R-free | 0.24050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vy2 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.460 |
High resolution limit [Å] | 2.320 | 2.320 |
Rmerge | 0.100 | 0.490 |
Number of reflections | 24528 | |
<I/σ(I)> | 10.08 | 2.64 |
Completeness [%] | 99.1 | 97.2 |
Redundancy | 3.78 | 3.78 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 20 %(V/V) MPD, 0.05 M MES, PH 5.6, 0.1 M MAGNESIUM ACETATE |