4B8E
PRY-SPRY domain of Trim25
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-11 |
Detector | ADSC CCD |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 58.149, 73.561, 91.009 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.505 - 1.779 |
R-factor | 0.1744 |
Rwork | 0.173 |
R-free | 0.19440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wl1 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.998 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 91.010 | 1.880 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.050 | 0.610 |
Number of reflections | 38142 | |
<I/σ(I)> | 20.9 | 3.5 |
Completeness [%] | 99.8 | 99.2 |
Redundancy | 7.2 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% PEG 3350, 0.2M NACL, 0.1M TRIS-HCL PH 8.5 |