4AZS
High resolution (2.2 A) crystal structure of WbdD.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 159.220, 159.220, 159.220 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 65.000 - 2.150 |
| R-factor | 0.1786 |
| Rwork | 0.176 |
| R-free | 0.22168 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.679 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 65.000 |
| High resolution limit [Å] | 2.200 |
| Rmerge | 0.090 |
| Number of reflections | 36526 |
| Completeness [%] | 100.0 |
| Redundancy | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
