4AI9
JMJD2A Complexed with Daminozide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-09-17 |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 100.476, 149.752, 57.533 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.620 - 2.250 |
R-factor | 0.216 |
Rwork | 0.216 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ox0 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.620 | 2.330 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.110 | 0.640 |
Number of reflections | 40190 | |
<I/σ(I)> | 10.4 | 2.2 |
Completeness [%] | 95.6 | 96.6 |
Redundancy | 3.4 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 277 | 0.1M CITRATE PH 5.5, 4MM NICL2, 20% PEG 3350, VAPOUR DIFFUSION, SITTING DROP, TEMPERATURE 277K |