4ADL
Crystal structures of Rv1098c in complex with malate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 271.530, 98.130, 90.000 |
Unit cell angles | 90.00, 101.34, 90.00 |
Refinement procedure
Resolution | 22.180 - 2.200 |
R-factor | 0.155 |
Rwork | 0.154 |
R-free | 0.17810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3no9 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.010 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.840 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.120 | 0.430 |
Number of reflections | 116132 | |
<I/σ(I)> | 7.6 | 2.7 |
Completeness [%] | 98.1 | 93.3 |
Redundancy | 3.3 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |