4ACH
GSK3b in complex with inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 173 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.949, 85.167, 178.389 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.940 - 2.600 |
R-factor | 0.2313 |
Rwork | 0.230 |
R-free | 0.25170 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.150 | 0.780 |
Number of reflections | 38939 | |
<I/σ(I)> | 5.4 | 1.1 |
Completeness [%] | 97.6 | 99.5 |
Redundancy | 2.7 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |