4AC9
CRYSTAL STRUCTURE OF TRANSLATION ELONGATION FACTOR SELB FROM METHANOCOCCUS MARIPALUDIS IN COMPLEX WITH GDP
Replaces: 1WB1Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-02-21 |
Detector | MARRESEARCH MAR165 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 146.920, 146.920, 297.480 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.975 - 3.030 |
R-factor | 0.1913 |
Rwork | 0.190 |
R-free | 0.22210 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.004 |
RMSD bond angle | 0.978 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CNS |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.210 |
High resolution limit [Å] | 3.030 | 3.030 |
Rmerge | 0.120 | 1.270 |
Number of reflections | 139069 | |
<I/σ(I)> | 14.37 | 2 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 8 | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10 MM KCL,20 MM TRIS/HCL (PH 7.5),40 MM MGSO4,2 MM DTT,3 MM GDP,1.8 - 2.0 M AMMONIUM SULFATE,100 MM SODIUM CITRATE (PH 6.0),1 MM DEOXYCHOLIC ACID. |