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4A1G

The crystal structure of the human Bub1 TPR domain in complex with the KI motif of Knl1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-1
Synchrotron siteESRF
BeamlineID14-1
Temperature [K]100
Detector technologyCCD
Collection date2009-07-07
DetectorADSC QUANTUM 210
Spacegroup nameP 1 21 1
Unit cell lengths59.279, 130.969, 74.956
Unit cell angles90.00, 110.17, 90.00
Refinement procedure
Resolution61.983 - 2.600
R-factor0.1889
Rwork0.186
R-free0.24360
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3esl
RMSD bond length0.009
RMSD bond angle1.173
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]65.0002.740
High resolution limit [Å]2.6002.600
Rmerge0.0700.500
Number of reflections32541
<I/σ(I)>13.73.2
Completeness [%]98.899.6
Redundancy2.82.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
161.25-1.3 M NA MALONATE, PH 6.0.

226707

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