4ZLT

Crystal structure of viral chemokine binding protein R17 in complex with CCL3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 4.2.2
Synchrotron site	ALS
Beamline	4.2.2
Temperature [K]	100
Detector technology	CCD
Collection date	2013-06-13
Detector	NOIR-1
Wavelength(s)	1
Spacegroup name	I 2 2 2
Unit cell lengths	98.493, 109.482, 210.956
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.247 - 3.000
R-factor	0.2195
Rwork	0.215
R-free	0.27400
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4ZKQ and 2X6G
RMSD bond length	0.003
RMSD bond angle	0.462
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	49.200	3.680
High resolution limit [Å]	2.761	19.680	2.780
Number of reflections	26825
<I/σ(I)>	7.4
Completeness [%]	100.0
Redundancy	4.7		1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		297	15-20% PEG 3350 0.2-0.4M MgFormate