4ZIC
Crystal Structure of Aspartate Semialdehyde Dehydrogenase with NADP from Trichophyton rubrum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97876 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 157.427, 157.427, 187.987 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.133 - 2.553 |
R-factor | 0.229 |
Rwork | 0.227 |
R-free | 0.27250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zhs |
RMSD bond length | 0.004 |
RMSD bond angle | 1.056 |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.710 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.056 | 0.336 |
Number of reflections | 168846 | |
<I/σ(I)> | 19.84 | 4.37 |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 3.84 | 3.83 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 293 | 0.15M Ammonium Sulfate, 0.1M Sodium Citrate, 15% PEG 4000 |