4YXL
Crystal structure of Syrian hamster prion protein complexed with POM1 FAB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-30 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97947 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 83.916, 105.969, 76.326 |
Unit cell angles | 90.00, 95.37, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 19709 | |
<I/σ(I)> | 15.46 | 1.44 |
Completeness [%] | 97.4 | 87.5 |
Redundancy | 4 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 25% PEG3350, 0.1 M BIS-TRIS, 0.2 M lithium sulphate |