4WVM
Stonustoxin structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-02-24 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.95659 |
| Spacegroup name | P 43 |
| Unit cell lengths | 107.911, 107.911, 244.345 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.150 - 3.100 |
| R-factor | 0.2086 |
| Rwork | 0.207 |
| R-free | 0.23640 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.120 |
| Data scaling software | XSCALE |
| Phasing software | SHELXDE |
| Refinement software | BUSTER (2.10.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.150 |
| High resolution limit [Å] | 3.100 |
| Number of reflections | 50233 |
| <I/σ(I)> | 11.72 |
| Completeness [%] | 99.1 |
| Redundancy | 4.59 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293.15 | 4.2 M NaCl |
