4WP5
Chaetomium thermophilum Mex67 NTF2-like domain complexed with Mtr2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-31 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 103.215, 103.215, 89.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.646 - 2.900 |
R-factor | 0.2222 |
Rwork | 0.221 |
R-free | 0.25400 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.701 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.700 |
High resolution limit [Å] | 2.900 |
Number of reflections | 12265 |
<I/σ(I)> | 11.4 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication for details |