4WCU
PDE4 complexed with inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | OTHER |
| Temperature [K] | 100 |
| Collection date | 2007-04-12 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 99.232, 113.545, 160.535 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 92.850 - 2.350 |
| R-factor | 0.2466 |
| Rwork | 0.244 |
| R-free | 0.30372 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.216 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 92.450 | 2.430 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Number of reflections | 70787 | |
| <I/σ(I)> | 8 | 2.4 |
| Completeness [%] | 93.1 | 92.1 |
| Redundancy | 4.36 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
