4V59
Crystal structure of fatty acid synthase complexed with nadp+ from thermomyces lanuginosus at 3.1 angstrom resolution.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 215.780, 412.670, 220.900 |
Unit cell angles | 90.00, 111.57, 90.00 |
Refinement procedure
Resolution | 12.000 - 3.100 |
Rwork | 0.270 |
R-free | 0.30000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.280 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.240 | 0.800 |
Number of reflections | 645016 | |
<I/σ(I)> | 6.5 | 2.3 |
Completeness [%] | 99.7 | 98.4 |
Redundancy | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.0 |