4UYZ
STRUCTURE OF THE WNT DEACYLASE NOTUM - CRYSTAL FORM II - 2.8A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Collection date | 2012-01-28 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.829, 193.880, 75.717 |
| Unit cell angles | 90.00, 91.88, 90.00 |
Refinement procedure
| Resolution | 96.940 - 2.800 |
| R-factor | 0.24899 |
| Rwork | 0.248 |
| R-free | 0.29294 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.267 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 58.000 |
| High resolution limit [Å] | 2.800 |
| Rmerge | 0.160 |
| Number of reflections | 38300 |
| <I/σ(I)> | 6.6 |
| Completeness [%] | 89.1 |
| Redundancy | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6 | pH 6.0 |
