4UO7
Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with 6SO4 Sialyl Lewis X
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 167.306, 348.485, 95.813 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 174.240 - 3.000 |
R-factor | 0.23516 |
Rwork | 0.233 |
R-free | 0.27595 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4uo4 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.229 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.720 | 3.210 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.100 | 0.470 |
Number of reflections | 53827 | |
<I/σ(I)> | 10.4 | 2.3 |
Completeness [%] | 95.6 | 95.6 |
Redundancy | 3.3 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |