4UHZ
Crystal structure of the human RGMB-BMP2 complex, crystal form 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-07 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 21 3 |
Unit cell lengths | 129.010, 129.010, 129.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.850 |
R-factor | 0.206 |
Rwork | 0.205 |
R-free | 0.22860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.030 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.930 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.050 | 0.820 |
Number of reflections | 8429 | |
<I/σ(I)> | 15.1 | 1.5 |
Completeness [%] | 99.4 | 98.9 |
Redundancy | 4.2 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2 M AMMONIUM SULPHATE, 8% (V/V) 2,5- HEXANEDIOL |