4UHW
Human aldehyde oxidase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 148.930, 148.930, 133.250 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 105.310 - 2.600 |
| R-factor | 0.19099 |
| Rwork | 0.189 |
| R-free | 0.23300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3zyv |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.286 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 74.460 | 2.690 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.260 | 1.180 |
| Number of reflections | 46600 | |
| <I/σ(I)> | 11.2 | 1.5 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 16.5 | 15.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
