4U58

IMPORTIN-ALPHA MINOR NLS SITE INHIBITOR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04-1
Synchrotron site	Diamond
Beamline	I04-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2011-11-05
Detector	PSI PILATUS 6M
Wavelength(s)	0.9686
Spacegroup name	P 21 21 21
Unit cell lengths	79.160, 90.630, 101.030
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	62.311 - 2.560
R-factor	0.2141
Rwork	0.211
R-free	0.26360
Data reduction software	XSCALE
Refinement software	PHENIX ((phenix.refine: dev_1702))

Data quality characteristics

	Overall
Low resolution limit [Å]	62.400
High resolution limit [Å]	2.560
Number of reflections	23793
<I/σ(I)>	13.5
Completeness [%]	97.5
Redundancy	5.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	see publication