4U3Z
APO MAP4K4 T181E Phosphomimetic Mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-15 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.720, 80.900, 92.570 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.407 - 2.090 |
R-factor | 0.186 |
Rwork | 0.183 |
R-free | 0.24900 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.081 |
Data scaling software | SCALA |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.000 | 2.200 |
High resolution limit [Å] | 2.090 | 2.090 |
Number of reflections | 36129 | |
<I/σ(I)> | 11.2 | 2.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.3 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 292 | 0.2 M potassium citrate, pH 8.3, 20% PEG 3350 |