4TQ0
Crystal structure of human ATG5-ATG16N69
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2012-03-06 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 93.094, 93.094, 245.577 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.092 - 2.697 |
R-factor | 0.2074 |
Rwork | 0.203 |
R-free | 0.27420 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.390 |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.697 |
Number of reflections | 28321 |
<I/σ(I)> | 39.1 |
Completeness [%] | 99.9 |
Redundancy | 15.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 400, MgCl2, KCl, Tris-HCl |