4S0H

TBX5 DB, NKX2.5 HD, ANF DNA Complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97670
Spacegroup name	P 1 21 1
Unit cell lengths	70.217, 78.459, 78.695
Unit cell angles	90.00, 108.83, 90.00

Refinement procedure

Resolution	38.164 - 2.817
R-factor	0.1946
Rwork	0.189
R-free	0.24750
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.387
Data reduction software	HKL-2000
Refinement software	PHENIX ((phenix.refine: 1.7.2_869))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	74.481
High resolution limit [Å]	2.817	2.817
Number of reflections	18168
Completeness [%]	99.9
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1