4PRG
0072 PARTIAL AGONIST PPAR GAMMA COCRYSTAL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1998-07-01 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 92.720, 61.540, 118.810 |
Unit cell angles | 90.00, 102.57, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.900 |
R-factor | 0.243 * |
Rwork | 0.240 |
R-free | 0.28300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 25.800 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (0.5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.700 |
Rmerge | 0.060 |
Number of reflections | 118972 |
Completeness [%] | 75.0 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 * | pH 7.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | Tris | 25 (mM) | |
3 | 1 | drop | dithiothreitol | 5 (mM) | |
4 | 1 | drop | 200 (mM) | ||
5 | 1 | drop | EDTA | 1.5 (mM) | |
6 | 1 | reservoir | PEG4000 | 15 (%) | |
7 | 1 | reservoir | HEPES | 100 (mM) |