Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-04-14 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 64 |
| Unit cell lengths | 94.568, 94.568, 85.825 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.000 - 2.300 |
| R-factor | 0.2051 |
| Rwork | 0.203 |
| R-free | 0.25370 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.414 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.1.29) |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.280 | 2.380 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.059 | 1.113 |
| Rpim | 0.020 | 0.382 |
| Total number of observations | 184048 | 17980 |
| Number of reflections | 19468 | |
| <I/σ(I)> | 27.1 | 2.3 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 9.5 | 9.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 20% PEG4000, 10% ISOPROPANOL, 0.1 M HEPES |
