4P5D
CRYSTAL STRUCTURE OF RAT DNPH1 (RCL) WITH 6-NAPHTHYL-PURINE-RIBOSIDE-MONOPHOSPHATE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-03-09 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 178.200, 178.200, 56.922 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.165 - 2.110 |
R-factor | 0.1757 |
Rwork | 0.175 |
R-free | 0.19780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fyi |
RMSD bond length | 0.009 |
RMSD bond angle | 1.430 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.15) |
Phasing software | MOLREP (10.2.31) |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.590 | 2.220 |
High resolution limit [Å] | 2.109 | 2.110 |
Rmerge | 0.066 | 0.540 |
Number of reflections | 31129 | |
<I/σ(I)> | 15.9 | 3.9 |
Completeness [%] | 99.4 | |
Redundancy | 6.5 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 1.3 M LITHIUM SULFATE, 1% PEG2K, 20 MM MAGNESIUM SULFATE, 100 MM TRIS, PH 8.0 |