4P0W
Human farnesyl diphosphate synthase in complex with Arenarone and zoledronate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-F |
| Synchrotron site | APS |
| Beamline | 21-ID-F |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2013-12-13 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.97872 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 111.239, 111.239, 67.292 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.580 - 2.406 |
| R-factor | 0.2077 |
| Rwork | 0.204 |
| R-free | 0.28940 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.791 |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 57.580 |
| High resolution limit [Å] | 2.400 |
| Number of reflections | 16815 |
| <I/σ(I)> | 30.79 |
| Completeness [%] | 99.7 |
| Redundancy | 26 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 1.2M sodium potassium phosphate, 25% glycerol |
