4OYE
Crystal structure of GltPh R397A in apo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-07-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9700 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 112.365, 424.422, 113.985 |
Unit cell angles | 90.00, 119.38, 90.00 |
Refinement procedure
Resolution | 20.000 - 4.000 |
R-factor | 0.24993 |
Rwork | 0.249 |
R-free | 0.26648 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.393 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 4.000 |
Number of reflections | 52068 |
<I/σ(I)> | 12.3 |
Completeness [%] | 70.3 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG400 Choline chloride citrate/tris |