4LGK

X-ray structure of the adduct between hen egg white lysozyme and Au2Phen, a dinuclear gold(III) complex with -dioxo bridges linking the two metal centers

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Collection date	2013-02-11
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	77.435, 77.435, 37.191
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.350 - 1.960
R-factor	0.21506
Rwork	0.211
R-free	0.30032
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.021
RMSD bond angle	1.938
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall
Low resolution limit [Å]	26.800
High resolution limit [Å]	1.960
Rmerge	0.113
Number of reflections	7204
Completeness [%]	84.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1