4L47
Crystal Structure of Frameshift Suppressor tRNA SufA6 Bound to Codon CCC-U on the Ribosome
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-23 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 210.200, 450.230, 621.740 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.966 - 3.220 |
R-factor | 0.23075614842 |
Rwork | 0.229 |
R-free | 0.25983 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3I9D AND 3I9E |
RMSD bond length | 0.006 |
RMSD bond angle | 1.101 |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 34.966 | 3.260 | |
High resolution limit [Å] | 3.180 | 14.220 | 3.180 |
Rmerge | 0.249 | 0.016 | 0.016 |
Number of reflections | 962803 | 10555 | 70620 |
<I/σ(I)> | 7.88 | 38.28 | 1.08 |
Completeness [%] | 98.5 | 90.5 | 98.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 4% PEG 20k, 4% PEG550 MME, 0.1M TRIS-ACETATE, 0.2M KSCN, 10mM MgCl, pH 7.0, vapor diffusion, temperature 293K |