4KIK
Human IkB kinase beta
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 12.3.1 |
| Synchrotron site | ALS |
| Beamline | 12.3.1 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 110.954, 68.689, 107.401 |
| Unit cell angles | 90.00, 107.03, 90.00 |
Refinement procedure
| Resolution | 47.170 - 2.830 |
| R-factor | 0.1863 |
| Rwork | 0.184 |
| R-free | 0.23650 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.150 |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 47.200 |
| High resolution limit [Å] | 2.800 |
| Rmerge | 0.103 |
| Number of reflections | 34922 |
| <I/σ(I)> | 10 |
| Completeness [%] | 95.3 |
| Redundancy | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
