4IR9
Polymerase-DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-02 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.760, 57.040, 110.700 |
Unit cell angles | 90.00, 94.76, 90.00 |
Refinement procedure
Resolution | 47.660 - 2.330 |
R-factor | 0.21441 |
Rwork | 0.211 |
R-free | 0.27242 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.920 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.460 |
High resolution limit [Å] | 2.330 | 2.330 |
Rmerge | 0.061 | 0.514 |
Number of reflections | 44000 | |
<I/σ(I)> | 10 | 2.2 |
Completeness [%] | 99.5 | 99.5 |
Redundancy | 3.7 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 20% MPD , pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |