4GXL
The crystal structure of Galectin-8 C-CRD in complex with NDP52
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-18 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 76.087, 124.826, 43.737 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.818 - 2.023 |
R-factor | 0.1786 |
Rwork | 0.177 |
R-free | 0.21610 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.257 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.050 |
High resolution limit [Å] | 2.020 | 5.480 | 2.020 |
Rmerge | 0.085 | 0.043 | 0.333 |
Number of reflections | 13995 | ||
<I/σ(I)> | 11.7 | ||
Completeness [%] | 99.9 | 99 | 100 |
Redundancy | 5.3 | 4.8 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 283 | 2% PEG 400, 0.1M HEPES sodium pH 7.5, 2.0M ammonium sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 283K |