4ETW
Structure of the Enzyme-ACP Substrate Gatekeeper Complex Required for Biotin Synthesis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Detector technology | CCD |
| Detector | MARMOSAIC 300 mm CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 57.080, 57.210, 60.950 |
| Unit cell angles | 101.99, 90.10, 112.74 |
Refinement procedure
| Resolution | 35.130 - 2.050 |
| R-factor | 0.194 |
| Rwork | 0.192 |
| R-free | 0.23590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.195 |
| Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 42538 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
