4D4P
Crystal Structure of the Kti11 Kti13 heterodimer Spacegroup P65
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-11-07 |
| Detector | DECTRIS PILATUS 6M-F |
| Spacegroup name | P 65 |
| Unit cell lengths | 152.060, 152.060, 203.850 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 110.614 - 2.999 |
| R-factor | 0.2092 |
| Rwork | 0.208 |
| R-free | 0.23370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.559 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.080 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.010 | |
| Number of reflections | 53195 | |
| <I/σ(I)> | 17.05 | 1.23 |
| Completeness [%] | 99.6 | 94.9 |
| Redundancy | 11.39 | 11.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 100 MM TRIS PH 8.4, 2 M LI2SO4 |
