4CD3
RnNTPDase2 X4 variant in complex with PSB-071
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-01 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.230, 86.010, 140.070 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.760 - 2.190 |
R-factor | 0.18202 |
Rwork | 0.180 |
R-free | 0.23591 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.019 |
RMSD bond angle | 2.022 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.150 |
Number of reflections | 26244 |
<I/σ(I)> | 8.5 |
Completeness [%] | 100.0 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |