4CC0
Notch ligand, Jagged-1, contains an N-terminal C2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-24 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 55.980, 60.250, 62.650 |
Unit cell angles | 92.59, 104.44, 106.67 |
Refinement procedure
Resolution | 30.190 - 2.320 |
R-factor | 0.219 |
Rwork | 0.218 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.190 |
Refinement software | BUSTER (2.11.4) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.190 |
High resolution limit [Å] | 2.320 |
Rmerge | 0.140 |
Number of reflections | 31717 |
<I/σ(I)> | 4.3 |
Completeness [%] | 97.3 |
Redundancy | 1.77 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |