4C9E
Mouse ZNRF3 ectodomain in complex with Xenopus RSPO2 Fu1-Fu2 (Seleno Met) crystal form II
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-03-03 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 |
| Unit cell lengths | 70.991, 71.279, 72.109 |
| Unit cell angles | 69.29, 61.48, 84.31 |
Refinement procedure
| Resolution | 35.370 - 3.000 |
| R-factor | 0.24977 |
| Rwork | 0.245 |
| R-free | 0.33378 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.509 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 35.340 |
| High resolution limit [Å] | 3.000 |
| Rmerge | 0.070 |
| Number of reflections | 22849 |
| <I/σ(I)> | 6.4 |
| Completeness [%] | 98.6 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
