4C2W
Crystal structure of Aurora B in complex with AMP-PNP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 2M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.922, 66.656, 116.903 |
| Unit cell angles | 90.00, 96.83, 90.00 |
Refinement procedure
| Resolution | 43.770 - 1.700 |
| R-factor | 0.15841 |
| Rwork | 0.156 |
| R-free | 0.19534 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.198 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.600 | 1.790 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.030 | 0.140 |
| Number of reflections | 74825 | |
| <I/σ(I)> | 30.8 | 10 |
| Completeness [%] | 97.1 | 94 |
| Redundancy | 5.7 | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
