4BTS
THE CRYSTAL STRUCTURE OF THE EUKARYOTIC 40S RIBOSOMAL SUBUNIT IN COMPLEX WITH EIF1 AND EIF1A
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-07-01 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 209.990, 471.550, 298.540 |
Unit cell angles | 90.00, 91.02, 90.00 |
Refinement procedure
Resolution | 49.749 - 3.703 |
R-factor | 0.2021 |
Rwork | 0.202 |
R-free | 0.22940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2XZM |
RMSD bond length | 0.006 |
RMSD bond angle | 1.186 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.930 |
High resolution limit [Å] | 3.700 | 3.700 |
Rmerge | 0.150 | 0.770 |
Number of reflections | 607573 | |
<I/σ(I)> | 7.69 | 1.66 |
Completeness [%] | 99.0 | 97 |
Redundancy | 3.1 | 2.94 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.7 | 0.1 M MOPS-KOH PH 7.7, 0.1 M AMMONIUM SULPHATE, 7.5% PEG 8K, 1MM PUTRESCINE |