4BTK
TTBK1 in complex with inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 4r |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 170.940, 40.280, 50.270 |
| Unit cell angles | 90.00, 104.24, 90.00 |
Refinement procedure
| Resolution | 82.840 - 2.000 |
| R-factor | 0.1922 |
| Rwork | 0.190 |
| R-free | 0.24920 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 82.800 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.120 | 0.640 |
| Number of reflections | 21626 | |
| <I/σ(I)> | 8.2 | 2.2 |
| Completeness [%] | 95.3 | 92 |
| Redundancy | 5.3 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
