4BJ1
Crystal structure of Saccharomyces cerevisiae RIF2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-17 |
Detector | MARRESEARCH |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 78.360, 78.360, 236.210 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.650 - 2.940 |
R-factor | 0.1986 |
Rwork | 0.197 |
R-free | 0.22860 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.160 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | SHARP |
Refinement software | BUSTER (2.11.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.500 | 2.950 |
High resolution limit [Å] | 2.940 | 2.940 |
Rmerge | 0.050 | 0.540 |
Number of reflections | 9796 | |
<I/σ(I)> | 23.8 | 3.4 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 7.9 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 14-20% 1,4-BUTANEDIOL, 100 MM NA ACETATE PH 5.1 |