4AZS

High resolution (2.2 A) crystal structure of WbdD.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	I 2 3
Unit cell lengths	159.220, 159.220, 159.220
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	65.000 - 2.150
R-factor	0.1786
Rwork	0.176
R-free	0.22168
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.013
RMSD bond angle	1.679
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	65.000
High resolution limit [Å]	2.200
Rmerge	0.090
Number of reflections	36526
Completeness [%]	100.0
Redundancy	11

Crystallization Conditions

crystal ID	method	pH	temperature	details
1